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Beilstein J. Org. Chem. 2010, 6, No. 18, doi:10.3762/bjoc.6.18
Graphical Abstract
Figure 1: Structures of pentasaccharides 1 and 2.
Scheme 1: Preparation of pentasaccharide 8. 1) MeOH, acidic ion exchange resin; 2) Ac2O, pyridine; 3) 80% HOA...
Scheme 2: Preparation of pentasaccharide 14. 1) MeOH, acidic ion exchange resin; 2) Ac2O, pyridine; 3) 80% HO...
Figure 2: Roman numbering of saccharide units in all pentasaccharides for NMR assignment.